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 IAAC equipment


 

detail_main_220x290.jpg Stoe StadiP double measuring site

Type:                                         

X-ray powder diffractometer with Transmission/Debye-Scherrer goniometers, Mythen 1K strip detector and linear position sensitive detector (PSD)
Samples: Transmission measurement with flat specimen; Debye-Scherrer measurements with capillary specimens for air and moisture sensitive samples
Source / optics: Molybdenum sealed tube, Ge(111) monochromator
Accessories: Capillary sample holder, transmission sample holder for flat specimen, low temperature attachment (Oxford Cryosystems Cryostream 700)
Typical application: Phase analysis, determination of cell parameters (indexing), Rietveld refinement, temperature dependent measurements
Responsible Operator: Dr. Thilo Ludwig
Institut für Anorganische und Analytische Chemie
Additional information:

Technical specs (goniometer)

Technical specs (detector)

 

 

detail_main_220x290.jpg Stoe StadiP IP
Type: X-ray powder diffractometer with Transmission/Debye-Scherrer goniometer and image plate detector (IP; range: 140°)
Samples: Transmission measurements with flat specimen for fast measurements with image plate detector
Source / optics: Copper sealed tube, Ge(111) monochromator
Accessories:

Capillary sample holder, transmission sample holder for flat specimen, automatic transmission sample changer for up to 30 samples

Typical application: Phase analysis, determination of cell parameters (indexing)
Responsible Operator: Dr. Thilo Ludwig
Institut für Anorganische und Analytische Chemie
Additional information: Technical specs (goniometer)
Technical specs (detector)

 

 

P4 Stoe Stadi P
Type:                                            X-ray powder diffractometer with Transmission/Debye-Scherrer goniometer and linear position sensitive detector (PSD)
Samples: Transmission measurement with flat specimen; Debye-Scherrer measurements with capillary specimens for air and moisture sensitive samples
Source / optics: Copper sealed tube, Ge(111) monochromator
Accessories:

Capillary sample holder, transmission sample holder for flat specimen, automatic transmission sample changer for up to 30 samples

Typical application: Phase analysis, determination of cell parameters (indexing)
Responsible Operator: Dr. Thilo Ludwig
Institut für Anorganische und Analytische Chemie
Additional information: Technical specs (goniometer)
Technical specs (detector)

 

 

FMF equipment


 

d5000_main_600x800.jpg

Siemens D5000
Type:                                            

2-circle diffractometer with linear position sensitive detector

Samples:

Capillary samples or flat powder samples

Source / optics:

Copper sealed tube with Ge(111) monochromator and collimator

Accessories:

Capillary sample holder, sample holder for transmission mode, preparation: powder samples for transmission mode, preparation of capillary

Typical application:

Phase identification of powder samples

Responsible Operator:

Sebastian Schütt

Freiburger Materialforschungszentrum (FMF)

Additional information:

User manual (consulting responsible operator)